00511
| No. | Parameters | Kettle | Jacket | |
| 1 | Full volume（L） | 100 | ||
| 2 | Work volume（L） | 70 | ||
| 3 | Design pressure（MPa） | -0.1~1.1 | ATM | |
| 4 | Work pressure（MPa） | -0.09~0.9 | ATM | |
| 5 | Design temperature（℃） | 200 | 200 | |
| 6 | Work temperature（℃） | 150 | 150 | |
| 7 | Material | S31603、16Mn | Q345R | |
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Reaction Vessel:
In practice, we would suggest customers use SS 31603 only because the area of the cladding plate used in this case is very little not help cost saving too much. However, since the rigidity of carbon steel is necessarily required, the cladding plate is used here. Open type The vessel is using open type to help with the maintenance and cleaning of the vessel. |
Medium transportation parts:
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| Agitator: It is roughly made from 4 components: An explosion-proof variable frequency motor, reducer, magnetic shaft, and paddles.
So, it helps the researcher to test the mixing conditions at various speeds. The explosion-proof feature of this motor ensures the safety of operation and prevents it from explosion.
Propeller and inclined blade paddle. The propeller at the top side will push the fluid downward, while the inclined blade paddle at the downside will push the fluid upward. So, there will be a good effort of fluid mixing caused by them which helps the inlet gas mix evenly with the fluid. |
Temperature control components: It consists of cooling components (the coil and cooling water inlet pipe), heating components (Electric heating bar, jacket, bath oil inlet & outlet ports, and pipes), and an insulation layer.
The PID controller not only monitors the temperature but also the stirring speed, the pressure inside the vessel, and the current inside the motor. When maintenance is needed, the lifting rack will hang the reactor lid up, till the paddles of the agitator are totally out of the vessel's cylinder. Then the maintenance will be done. After the maintenance is finished, the reactor lid will be put back in position and fixed with bolts. To ensure the sealing effort, the reactor uses using flange fixture, graphite gasket, and gaskets for other nozzle ports. We have also prepared several pcs of them as spare parts for future consumption.
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1.1 Brief description of the structure of the Pilot Reaction and Distillation System.This reaction and distillation reactor is an essential part of the pilot experiment system being used by our pharmaceutical client.To the left side of the reactor is the lifting rack, which is driven by an electric motor to pull the lifting rope to open the lid of the reactor. To the right side of the reactor is the end product condenser and collecting system (not shown in this picture), which is installed and under service at the client's site. All of the above three parts make up the pilot reaction and distillation system. 1.2 Components of reactor:Agitator.Reaction Vessel. Temperature control componnets. Medium transportation parts. Support. |
| Items | Vessel | Jacket | Coil |
| Design Pressure / Mpa | -0.1~1.1 | Atmospheric | 0.5 |
| Work Pressure / Mpa | -0.09~0.9 | Atmospheric | 0.4 |
| Design Temperature / ℃ | 200 | 200 | 200 |
| Work Temperature / ℃ | Room temperature to 200 | Room temperature to 200 | Room temperature to 200 |
| Medium | Bath oil | Water | |
| Material | SS 31603 + Carbon Steel Q345R | Q345R | SS 31603 |
| Paddles type | Propeller +Inclined-blade mixing paddle | ||
| Shaft sealing | Magnetic sealing | ||
| Power of motor / KW | 1.5 | ||
| Strirring Speed / RPM | 0~600 | ||
| Heating method | Electric bar | ||
| Application | Pharmaceutical industry pilot experiment | ||
