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  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system
  • WHGCM 100L stainless steel 304 polycondensation reactor with distillation system

WHGCM 100L stainless steel 304 polycondensation reactor with distillation system

No.00387
Pilot reactor +stainless steel + Composite plate polycondensation reactor , 100L, high-speed stirring, with jacket Mechanical seal Explosion-proof corrosion-resistant reactor with heat preservation Stirrer with balance tank Vacuum, Open type Intelligent control
No. Parameters Kettle Jacket
1 Full volume(L) 150
2 Work volume(L) 100
3 Design pressure(MPa) -0.1~1.6 ATM
4 Work pressure(MPa) -0.1~1 ATM
5 Design temperature(℃) 320 320
6 Work temperature(℃) 280 280
7 Material S30408,16Mn Q345R
Description

poster of the 100L pilot scale polycondensation reactor

Title of product introductionTitle of product structure
Picture of 100L pilot scale polycondensation reactor  structure
1. One set of explosion-proof PID intelligent controller, the parameters are controllable and adjustable (frequency control, motor current display, temperature display, heating temperature control) temperature control accuracy of ± 1 ℃.
2. One set of vertical magnetic coupler (bushings with a backup), with explosion-proof motor. With explosion-proof electric heater, heat conduction oil.
3. Valves, vacuum gauge, pressure gauge, rupture disc, explosion-proof platinum resistance, feeding port with blind, with sight glass, under the discharge port with wire plug, with heating with casting with head, heating temperature 220-230 ° C, casting with the head of the 6 5mm holes, hole spacing of 10-15mm, (another with a ball valve, remove the wire plug can be connected to the bottom of the kettle with), with wrenches, gaskets (feeding mouth) Gasket with a gasket for two, kettle cover gasket with a gasket for one), standard accessories.
Condensing port with condenser three pieces, 50L collection tank 2 pieces (sight glass open in the lower head), 25L buffer tank 1 piece, including connecting pipe fittings and valves, material are stainless steel S30408.
4.
Materials: 
Inner cylinder head material is stainless steel S30408, 
flange jacket material 16Mn, 
insulation cylinder material is stainless steel, 
kettle cover with insulation, 
insulation shell material stainless steel.
5. With one ZX-15L explosion-proof vacuum pump, including connecting pipeline. The no-load vacuum degree is required to reach within 50Pa.
6. with electric lifting device (motor explosion-proof), kettle cover fixed kettle body electric lifting (power 1.5-2KW), electric flip (power 1.5-2KW). The material is carbon steel spraying.
7.With a discharge cooling water tank.
8. Nameplate, control panel, and manual are all in English Version.
9.Voltage: 380V

Title of product Features
This is pilot reactor for polycondensation. 
Reaction kettle: 
Profile:
Open style, conical bottom.
The coincal bottom could help the discharging with high viscosity.
Material:
stainless steel S304.
Cylinder size:
ᆞDia. 500mm * H550mm.  
ᆞThickness 6mm.
This size lets a 150 liters full volume of the kettle, and allows a 100 liters work volume for the reaction.
Main flange:
Material is S304 surfacing welded carbon steel 16Mn.
Its size is designed as per the pressure and temperature.
The main flange is usually applied for the reactor with open style. The reactor would be opened when the reaction is finished, or for maintaining. 
Agitator:
Motor:
ᆞExproof. The monomer of the reaction is flammable. Besides the motor , the other parts such as electric heaters, motor for lifting, also need Exproof feature.
ᆞPower: 4KW.
It offers enough stirring torque for the large blade.
Reducer:
It ensure the stirring speed to be 200RPM max.
Magnetic shaft sleeve coupler:
ᆞIt is long enough for containing the magnetic rings inside the sleeve for big torque.
ᆞIt is using ciculating water for the magnetic rings cooling.
Shaft coupler
ᆞBecause the large torque caused to the shaft by the polycondensation product, this part is also needed.
Two layers mixer with paddle and Anchor frame blades:
This kind of design could ensure uniform mixing of the monomer and polycondensation product mixture.
The bottom shape of the anchor frame is simliar with the conical bottom of kettle, so the polycondensation product could be fully stirred by it.
Material:
Stainless steel S304.
The medium has slightly corrosion, so all the material of the agitator parts that contact the medium are S304. 
Jacket:
Temperature adjusting jacket
This jacket is attached outside of the kettle wall. It works together two parts to adjust the temperature of thermal oil inside it.
One is the electric heaters injected from its bottom, the other is the cooling coils with the inlet/outlet ports opened on its bottom too.
ᆞThe heater is used to start the condensation reaction after the medium charged into the kettle.
ᆞAnd the cooling coils is to cool the temperature at certain temperature, to prevent the reaction temperature become too high to control. As the condensation reaction is exothermic reaction that it is easy to runaway.
Insulation Jacket
This jacket is assembled outside of the temperature adjusting jacket. It is used to prevent the heat escaping. 
Condensers:
There are three condensers in this set of contraption. 
Vertical condenser:
It is used to expel the unnecessary gas phase by-product of the consensation reaction. 
The length of heat exchange tube is 800mm, which ensure the medium needed by the consensation could be cooled down and reflux in liquid phase.
Horizontal condensers:
These two condensers are design to recover the by-products after the condensation.
The by-products will be collected by the receiving tanks.

Specification

Design pressure (MPa) Working pressure (MPa) Design Temperature (℃) Operating temperature (℃)
Kettle -0.1~1.6 -0.1~1 320 280
Jacket ATM ATM 320 280
Material Stirring mode Stirring speed Heating method
Kettle S30408,16Mn anchor frame 0~200 oil bath electric heating
Motor power (W) Sealed manner corrosion allowance joint efficiency
Kettle 4KW(dIIBT4) magnetic force 1 1


pilot reactor general parameters range form
Piture of optional accessoriesTitle of WHGCM Manufacturing capaciptyTesting and producing machines in WHGCMcases and customers photoWHGCM packing and shipping photo

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