00617
| No. | Paramters | Left reactor | Right reactor | |
| 1 | Full volume（L） | 4.2 | ||
| 2 | Work volume（L） | 3.0 | ||
| 3 | Design pressure（MPa） | -0.1 | -0.1 | |
| 4 | Work pressure（MPa） | -0.1 | -0.1 | |
| 5 | Design temperature（℃） | 100 | 300 | |
| 6 | Work temperature（℃） | 80 | 250 | |
| 7 | Material | S304 | S316L | |
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| Structure: This pilot plant consists of two sets of reactors with distillation contraptions, two sets of charging contraptions and an intelligent controller. Flow diagram: The flow starts at the left reactor. Because the reactors are series connected, the product of right reactor will be charged to the right reactor as its reactant. The finial product is collected at the receiving tank of right distillation contraption. The charging of the medium is automaticly contolled by the controller, so the whole process is continuous. |
Reactors: The low temperature reactor ( Left ) Work temperature: 80°C Material: Stainless steel 304. The high temperature reactor ( right ) Work temperature: 250°C Material: Stainless steel 304. Both of them with the kettle size of 3L. They are double jacketed designed, one heating jacket with electric heated. The other is insulation jacket filled with rock wool. |
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| Distillation equipments: The distillation contraption including the a mini vertical condensing column and a collecting tank. Distillation columns: ᆞ Left one: Material: Stainless steel 304. Size: Dia. 55* H500. Cooling type: air cooling. Stilling time: None. Product phase：Gas. ᆞ Right one: Material: Stainless steel 316L. Size: Dia. 55* H500. Cooling type: water cooling. Stilling time: 40 mins. Porduct phas: liquid. Collection tank: Material: S316L. Size: 30L. The by-product of right reactor will get into the left collecting tank and be weighed there. |
The other parts: Charging unit: The charging contraption is two constant pressure charging tanks. Rack: All of the deives are supported by the stainless steel rack, which makes the pilot plant compact and good looking. Other parts: ᆞ Vaccum pumps: They are to vacuum the system for distillation. ᆞ PLC controller: The parameters including temperature, pressure, and stirring speed are displayed and monitered. The programe is well designed to realize the automation running of the pilot plant. In addition, the PLC is integrated data transceiver, can be monitored and controlled from a remote computer or smartphone. In this way, it is also named Remote real-time control of reactor systems. |
