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  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor
  • 100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor

100 ml micro stainless steel high pressure PTFE hydrothermal synthesis reactor

No.00400
It is mainly all-metal arc surface seal, made of GB 316L stainless steel.
It is suitable for digestion of samples with high requirements for temperature and pressure and general corrosivity.
Description

I Specification

Volume: 100 ml
Model: SL 100
Material: 316L stainless steel
Pressure: 10 Mpa
Temperature: 400 ℃
Structure: snap ring quick disassembly mode
Sealing method: A type double seal

II Advantages of microreactor: 

The reaction is able to proceed quickly at high pressure.
No loss of analytical samples or trace elements during dissolution.
No additional ingredients are added to affect product analysis.

III Other types

3.1 Volume for choosing:

10ml,25ml, 50ml, 100ml,200ml,300ml

3.2 Highest pressure

50Mpa

3.3 Highest temperature

600 degree Celsius  ( 1112 degree fahrenheit)

3.4 Material for choosing:

Stainless steel 316L, Hastelloy C276, zirconium alloy, titanium alloy, tantalum alloy and so on.

IV Tips for using

4.1 Circumstance

Before opening or closing the kettle body, be sure to put it on the disassembly plate to fix it.

4.2 Opening processes

4.2.1 Open the gas relief valve to vent internal pressure 
4.2.2 Loosen the screws on the snap ring, then loosen the retaining nut on the snap ring and lower the snap ring onto the table.
4.2.3 Remove the two snap rings and lift the lid with all the accessories out of the kettle body.
4.2.4 Move the lid carefully so as not to damage the mixing shaft and other accessories during removal.

4.3 Closing processes

4.3.1 Slide the two snap rings into place so that the grooves drilled in the outer surface of the snap rings are at 180 ℃ on the gauge head.
4.3.2 Raise the ferrule to the outer surface of the snap ring, adjust the position so that the set screw enters the groove above, and then tighten the screw slightly to position the ferrule.
Check the joint surfaces of lid and kettle body to ensure they are smooth and free of bumps, and then put lid on kettle body.
Please note:
A Carefully inspection on the gasket in the lid need to be done, making sure it is intact before closing the kettle.
There would be having thin irregular burrs outward on the inner and outer radial edges of the gasket , after several times of using. It does not mean that the gasket needs to be replaced. You could remove the burrs with a sharp knife.
4.3.3 Seal. 
Tighten each screw with the wrench provided, and apply a stable and strong clamping force to each screw.
If you're using torque wrench, then enforce each screw to 25 ft-lbs.
Tighten screws in a criss-cross fashion rather than counterclockwise.
After initial tightening, allow the kettle body to withstand pressure and tighten again. This will compensate for the tendency of the gasket to expand under applied pressure.
4.3.4 Place the kettle body on the bracket with the head facing forward and insert the set screw on the ferrule into the hole in the metal plate on the bracket.This prevents the kettle from rotating while stirring.
4.3.5 Raise the heater flush with the lower edge of the kettle bracket.

V Introduction of micro synthesis reactor:

5.1 Strict material selection: 

Materials are crucial to the durability and reliability of the synthesis kettle, similar materials have several times the price difference.
In order to make sure the kettle is reliable and durable, all synthesis kettle are made of superior materials.

5.2 New sealing structure design; 

Comparing with traditional structure, whose polytetrafluoroethylene (PTFE) may be transformed during re-cooling process and causes leakage.
The hydrothermal kettle made by WHGCM maintain best sealing in the continuous high temperature and cooling process. 

5.3 Hole fastening tools tighten the seal, saving time and effort.

The autoclave has PTFE liner cover in constant tightening pressure in the whole process of reaction, thus promises good sealing performance.

5.4 High pressure resistance: 

Design pressure is 30Mpa.

VI Other name of this type of reactor

micro-synthesis reactor 
high temperature and high pressure hydrothermal kettle
high pressure digestion tank
sample dissolver
mini pressure vessel 
digestion tank
PTFE high pressure tank
non-stirred reactor
hydrothermal reactor
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